Investigating the cooling rate of cane molasses as quenching medium for 0.61% C high carbon steels
DOI:
https://doi.org/10.30544/139Keywords:
Martensite, Quenching, Cane Molasses, Viscosity, Cooling Rate, High Carbon SteelsAbstract
The effect of cooling rate of cane molasses as quenching medium for 0.61% C high carbon steels was investigated. Samples of high carbon steel were spheroidized annealed and then machined prior to the hardening process. Molasses solution of viscosity equals to that of engine oil was prepared by adding water. The samples were normalized and then austenitised at 800oC and soaked for 40 minutes and then quenched in water, engine oil, raw molasses and the prepared molasses solution. Cooling rate curves of all the quenching media used were developed. The highest cooling rate of 60oC/s was attained by the prepared molasses solution. Hardness of the test samples was evaluated. The test results obtained show that the highest hardness value (525 HVN) was obtained from the sample quenched in the prepared molasses solution. Microstructures of the various samples were analyzed using OM and SEM. In all the tests samples martensite structure was observed. It was observed that the prepared molasses solution has higher severity of quenching than that of engine oil but lower than that of water. The research showed that cane molasses can harden high carbon steel without cracking the component in the same way as engine oil, hence, molasses could be a very good alternative to engine oil for use as quenching medium.
References
E. Keehan, Effect of microstructure on mechanical properties of high strength steel weld metals, Ph.D. thesis, Dept. of Physics, Chalmers University of Technology, Sweden, 2004.
T.O Joshua, O.A Alao, R.T. Oluyori, Int. J. .Eng. Adv. Technol. 3 (2014), 121-127.
G.E. Totten, Steel Heat Treating Metallurgy and Technologies, Taylor and Francis Group LLC, Oregon, USA, 2006.
D.A. Fadare, T.G. Fadara, O.Y. Akanbi, J. Miner. Mater. Charact. Eng. 10 (2011) 299-308.
G.Totten, M.T. Hans, S. Anton, Quenching and quenching technology-steel heat treatment.(2ndEd), Taylor and Francis Group LLC, Boca Raton, Florida, 2006.
L. Olson, In: Proceedings 5. Physical Metallurgy: principle and practice, New Delhi: Prentice-Hall of India ltd. 1989.
B.A. Joseph, A.K. Oladiran, M. Edeki, B.A. Michael, A.A Samuel,J. Miner. Mater. Charact. Eng. 10 (2015) 85-93
C.C. Jensen, http://www.cjc.dk/index.php? m=p&pid=212, 30 March 2016.
B.O. Solomon, S.K. Layokun, T.O. Omobuwajo, Ife J. of Technol. 3 (1991) 25-29.
V.C. Leo, Molasses general consideration, West Des Moines,: National Feed Ingredients Assoc. Iowa, 1983.
S.O. Balogun, Potential of Cassava Liquid Extract as Quenching Medium for medium Carbon and Low alloy Steels, An M.Sc Thesis, Zaria: Department of Metallurgical and Material Engineering, Ahmadu Bello University, 2008.
T. Ause Evaluation of Hot Bitumen Bath as a Quenching Medium for Austempering of Steel and Ductile Cast Iron, A Ph.D Thesis, Zaria: Department of Metallurgical and Material Engineering, Ahmadu Bello University, 2007.
S.B. Hassan, J.B Agboola, V.S. Aigbodiun, E.J. Williams, Metall. Mater. Eng. 5 (2010) 31-36.
T.I. Muhammmad, Evaluation of Polymer Glycerol for Hardening Process in Steel and Cast Iron, Zaria: an M.Sc Seminar, Department of Metallurgical and Material Engineering, Ahmadu Bello University, 2007.
M. Saska, Boiling rate, heat transfer and viscosity of technical sugarcane liquors, Louisiana, USA: Audubon Sugar Inst., Louisiana State University Ag Center, St Gabriel.
O. R. Bodede, P.O. Ojo, O.R. Ayodele, A.F. Owa and O.B. Ajayi, J. Emerging Trends Eng. Appl. Sci. 3 (2011) 127-130.
S.B Hassan, S.O. Balogun, V.S. Aigbodion, Metall. Mater. Eng. 4 (2009) 55-61.
T. Vivek, P. Adarsh, M. Zuber, I.B. Chandrashekhar, Int. J. Innovative Res. Adv. Eng. 1 (2014), 46-49.
ASTM “Standard Test Method for Determination of Cooling Characteristics of Quench Oils by Cooling Curve Analysisâ€, ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428â€2959 USA, 2007.
ASTM “Standard Test Method and definitions for mechanical testing of steel productsâ€, ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428â€2959 USA, 2007.
W.D. Callister, Material Science and Engineering: An Introduction, John Wiley and Sons Inc., New York , 1997, 331-337.
C. S. Ester, F. O. Luiz, E. T George, C. F. Lauralice, J. Pet. Sci. Res. 2 (2013), 41-47.
Downloads
How to Cite
Issue
Section
License
Copyright (c) 2016 Metallurgical and Materials Engineering

This work is licensed under a Creative Commons Attribution 4.0 International License.
Authors who publish with this journal agree to the following terms:
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgment of the work's authorship and initial publication in this journal.
- Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgment of its initial publication in this journal.
- Authors are permitted and encouraged to post their published articles online (e.g., in institutional repositories or on their website, social networks like ResearchGate or Academia), as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access).
Except where otherwise noted, the content on this site is licensed under a Creative Commons Attribution 4.0 International License.