The Extraction of pure hydroxyapatite from porcine bone by thermal process
DOI:
https://doi.org/10.30544/410Keywords:
hydroxyapatite, porcine bone, thermal process, heating, biomaterialsAbstract
Natural hydroxyapatite (HA) has been extracted from porcine bone by thermal decomposition without any chemical treatment. The suitable condition to synthesize HA was chosen as a heating bone at 750 °C during 6 hours. XRD and FTIR analyses confirmed the high purity and crystallinity of synthetic HA. Furthermore, the transformation of the obtained HA to other phases did not mention up to 1200 °C. TG curve showed a slight loss of mass at 950 °C, but the DSC analysis did not present any physic-chemical phenomena during the period of measurement. FE-SEM images showed the different particles including spheres, scales, and rods in the structure of natural HA. EDX analysis indicated that the Ca/P ratio of the synthetic HA is 1.64, nearly the theoretical value of 1.67. Overall, the results obtained in this study confirmed the success of the thermal process to extract the natural HA from porcine bone.
References
J. Kolmas, S. Krukowski, A. Laskus, M. Jurkitewicz: Ceram Inter, 42 (2016) 2472-2487.
A. Rogina, M. Ivanković, H. Ivanković: Mater Sci Eng C, 33 (2013) 4539-4544.
W. Xiao, B. B. Sonny, M. N. Rahaman: Mater Sci Eng C, 60 (2016) 324-332.
Y. Suat: Ceram Inter, 44 (2018) 9703-9710.
Z. S. Stojanović, N. Ignjatović, V. Wu, V. Žunič, Lj. Veselinović, S. Škapin, M. Miljković, V. Uskoković, D. Uskoković: Mater Sci Eng C, 68 (2016) 746-757.
B. A. Ben-Arfa, I. M. Miranda Salvado, J. MF Ferreira, R. C. Pullar: Mater Sci Eng C, 70 (2017) 796–804.
M. N. Hassan, M. M. Mahmoud, A. A. El-Fattah, S. Kandil: Ceram Inter, l42 (2016) 3725-3744.
S. Beaufils, T. Rouillon, P. Millet, J. Le Bideau, P. Weiss, J. P. Chopart, A. L. Daltin: Mater Sci Eng C, 98 (2019) 333-346.
J. H. Seo, B. G. Hong: Nuc Eng Tech, 44 (2012) 9-20.
S. Ramesh, Z. Z. Loo, C. Y. Tan, WJ Kelvin Chew, Y. C. Ching, F. Tarlochan, Hari Chandran, S. Krishnasamy, L. T. Bang, A. A. Sarhan: Ceram Inter, 44 (2018) 10525-10530.
N. A. Barakat, M. S. Khil, A. M. Omran, F. A. Sheikh, H. Y. Kim: J Mater Process Tech, 209 (2009) 3408-3415.
A. Pal, S. Paul, A. R. Choudhury, V. K. Balla, M. Das, A. Sinha: Mater Lett, 203 (2017) 89–92.
C. F. Ramirez-Gutierrez, S. M. Londo-o-Restrepo, A. del Real, M. A. Mondragón, M. E. Rodriguez-García: Ceram Inter, 43 (2017) 7552-7559.
Hydroxyapatite Standard ICDD 9-432.
M. E. Bahrololoom, M. Javidi, S. Javadpour, J. Ma: J Ceram Process Res, 10 (2009) 129-138.
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2019 Bùi Xuân Vương, Truong Hoai Linh
This work is licensed under a Creative Commons Attribution 4.0 International License.
Authors who publish with this journal agree to the following terms:
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgment of the work's authorship and initial publication in this journal.
- Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgment of its initial publication in this journal.
- Authors are permitted and encouraged to post their published articles online (e.g., in institutional repositories or on their website, social networks like ResearchGate or Academia), as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access).
Except where otherwise noted, the content on this site is licensed under a Creative Commons Attribution 4.0 International License.
From the 2019 year, journal Metallurgical and Materials Engineering is indexed in 
According to the 